JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000465
Submitter
The Noguchi Institute
Reaction ID
R-0000-000466
Regist Date
2012/06/21 16:07:59
REACTANT
MOLECULE ID
JCGG-COM0000352 (Reaction Tree)
Reactant Type
ketopyranose
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000277
Reactant Type
Brφnsted acid
Mol
0.20 equiv.
PRODUCT
MOLECULE ID
JCGG-COM0000353 (Reaction Tree)
Product Type
anhydroketopyranose
Yield
59%
REACTION DETAIL
Reaction Time
30 hours
Reaction Temp
0 degree C
Solvent
MeCN
Catalyst
Brφnsted acid
Comment
CaSO4 was added to the solvent as a drying agent.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000019
Source
HETEROCYCLES, Vol. 82, No. 1, 2010, pp. -
Doi
10.3987/COM-10-S(E)24

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