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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000453 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000454
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Regist Date |
2012/06/21 16:07:28 | ||||
| REACTANT | |||||
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Reactant Type |
Substrate | ||||
Mol |
1 equiv. | ||||
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Reactant Type |
Nucleophile | ||||
Mol |
3 equiv. | ||||
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Reactant Type |
cat. | ||||
Mol |
0.2 equiv. | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
94% | ||||
| REACTION DETAIL | |||||
Reaction Time |
2 to 3 hours | ||||
Reaction Temp |
-78 degree C | ||||
Solvent |
MeCN-CH2Cl2(1:1) | ||||
Catalyst |
cat. | ||||
Comment |
CaSO4 was added to the solvent as a drying agent. | ||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| The anomer ratio was NOT specified. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000018 | ||||
Source |
SYNTHESIS 2007, No. 19, pp 3021-3031 | ||||
Doi |
10.1055/s-2007-983882 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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