|
Glycan Syntheses |
JCGG ID |
JCGG-RAC0000423 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000424
|
||||
Regist Date |
2012/06/21 15:57:45 | ||||
| REACTANT | |||||
|
|
|
||||
Reactant Type |
Substrate | ||||
Mol |
1 equiv. | ||||
|
|
|
||||
Reactant Type |
Nucleophile | ||||
Mol |
2 equiv. | ||||
|
|
|
||||
Reactant Type |
cat. | ||||
Mol |
0.2 equiv. | ||||
| PRODUCT | |||||
MOLECULE ID |
|
|
|||
Yield |
79% | ||||
MOLECULE ID |
|
|
|||
Product Type |
byproduct | ||||
Yield |
7% | ||||
| REACTION DETAIL | |||||
Reaction Time |
2 to 3 hours | ||||
Reaction Temp |
-20 degree C | ||||
Solvent |
MeCN | ||||
Catalyst |
cat. | ||||
Comment |
CaSO4 was added to the solvent as a drying agent. | ||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| The anomer ratio was NOT specified. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000018 | ||||
Source |
SYNTHESIS 2007, No. 19, pp 3021-3031 | ||||
Doi |
10.1055/s-2007-983882 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
|