JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000415
Submitter
The Noguchi Institute
Reaction ID
R-0000-000416
Regist Date
2012/06/21 15:57:20
REACTANT
MOLECULE ID
JCGG-COM0000406 (Reaction Tree)
Skeleton
JCGG-STR032525
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000420
Mol
2 equiv.
MOLECULE ID
JCGG-COM0000421
Mol
10 equiv.
MOLECULE ID
JCGG-COM0000418
Mol
3 equiv.
PRODUCT
MOLECULE ID
JCGG-COM0000407 (Reaction Tree)
Skeleton
JCGG-STR032525
Yield
94%
REACTION DETAIL
Reaction Time
5 hours, 48 hours
Reaction Temp
room temp, room temp
Solvent
THF, H2O
Comment
1) 9-BBN, THF, 2) H2O2 aq., 0.5 M NaOH aq., 94%
COMMENT
There are two phases in this reaction.
REFERENCE
Reference Id
REF-0000-000016
Issn
Print
PubMed ID
19122320
Journal Name
Chemical & pharmaceutical bulletin. (2009) 57 (1): 74-8.
Article Title
Syntheses and doxorubicin-inclusion abilities of beta-cyclodextrin derivatives with a hydroquinone alpha-glycoside residue attached at the primary side.
Author
Yoshiki, Oda; Masumi, Miura; Kenjiro, Hattori; Takashi, Yamanoi
Affiliation
The Noguchi Institute, Tokyo, Japan.
Reference Id
REF-0000-000017
Source
CHEMICAL & PHARMACEUTICAL BULLETIN, Vol. 57 (2009), No. 1, 74
Doi
10.1248/cpb.57.74

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)