JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000414
Submitter
The Noguchi Institute
Reaction ID
R-0000-000415
Regist Date
2012/06/21 15:57:17
REACTANT
MOLECULE ID
JCGG-COM0000417 (Reaction Tree)
Skeleton
JCGG-STR032525
Mol
3.7 mmol
MOLECULE ID
JCGG-COM0000418
Mol
4 mmol
MOLECULE ID
JCGG-COM0000419
Mol
4.8 mmol
PRODUCT
MOLECULE ID
JCGG-COM0000405 (Reaction Tree)
Skeleton
JCGG-STR032525
Yield
84%
REACTION DETAIL
Reaction Time
3 hours, 70 hours
Reaction Temp
room temp, room temp
Solvent
H2O, DMF
Comment
1) 0.5 M NaOH aq., H2O, 2) AllBr, DMF, 84%
COMMENT
There are two phases in this reaction.
REFERENCE
Reference Id
REF-0000-000016
Issn
Print
PubMed ID
19122320
Journal Name
Chemical & pharmaceutical bulletin. (2009) 57 (1): 74-8.
Article Title
Syntheses and doxorubicin-inclusion abilities of beta-cyclodextrin derivatives with a hydroquinone alpha-glycoside residue attached at the primary side.
Author
Yoshiki, Oda; Masumi, Miura; Kenjiro, Hattori; Takashi, Yamanoi
Affiliation
The Noguchi Institute, Tokyo, Japan.
Reference Id
REF-0000-000017
Source
CHEMICAL & PHARMACEUTICAL BULLETIN, Vol. 57 (2009), No. 1, 74
Doi
10.1248/cpb.57.74

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)