JCGG ID |
JCGG-RAC0000384 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-000384 | |||||||
Regist Date |
2012/06/21 15:47:28 | |||||||
REACTANT | ||||||||
|
|
|||||||
Reactant Type |
donor | |||||||
Mol |
1 equiv. | |||||||
|
|
|
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Reactant Type |
Alcohol | |||||||
Mol |
1 equiv. | |||||||
|
|
|||||||
Reactant Type |
activator | |||||||
Mol |
1 equiv. | |||||||
|
|
|||||||
Reactant Type |
activator | |||||||
Mol |
0.05 equiv. | |||||||
PRODUCT | ||||||||
MOLECULE ID |
|
|
|
|||||
Product Type |
alpha | |||||||
Yield |
52%(alpha/beta=23/77) | |||||||
MOLECULE ID |
|
|
||||||
Product Type |
beta | |||||||
Yield |
52%(alpha/beta=23/77) | |||||||
REACTION DETAIL | ||||||||
Reaction Time |
overnight | |||||||
Reaction Temp |
room temp | |||||||
Solvent |
PhH | |||||||
Catalyst |
activator | |||||||
Comment |
MS 4A was included in the solvent. | |||||||
COMMENT | ||||||||
The PMID could not be found. | ||||||||
The alpha/beta ratio was determined by the isolated yield. | ||||||||
REFERENCE | ||||||||
Reference Id |
REF-0000-000014 | |||||||
Source |
Bulletin of the Chemical Society of Japan, Vol. 67 (1994), No. 5 pp.1359-1366 | |||||||
Doi |
10.1246/bcsj.67.1359 |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |