JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000362
Submitter
The Noguchi Institute
Reaction ID
R-0000-000362
Regist Date
2012/06/21 15:40:32
REACTANT
MOLECULE ID
JCGG-COM0000136 (Reaction Tree)
Reactant Type
Donor
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000060
Reactant Type
Alcohol
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000032
Reactant Type
activator
Mol
1 equiv.
PRODUCT
MOLECULE ID
JCGG-COM0000382 (Reaction Tree)
Product Type
alpha
Yield
80%
REACTION DETAIL
Reaction Time
overnight
Reaction Temp
room temp
Solvent
PhH
Catalyst
activator
Comment
MS 4A was included in the solvent.
The reaction was sheltered from the light.
COMMENT
The PMID could not be found.
Only alpha was detected in the product.
The alpha/beta ratio was determined by 13C NMR spectroscopy.
REFERENCE
Reference Id
REF-0000-000014
Source
Bulletin of the Chemical Society of Japan, Vol. 67 (1994), No. 5 pp.1359-1366
Doi
10.1246/bcsj.67.1359

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)