JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
 JCGG-RAC0000360
Submitter
 The Noguchi Institute
Reaction ID
 R-0000-000360
Regist Date
 2012/06/21 15:40:26
REACTANT
MOLECULE ID
 JCGG-COM0000147 (Reaction Tree)
Reactant Type
 Donor
Mol
 1 equiv.
MOLECULE ID
 JCGG-COM0000043 (Reaction Tree)
Skeleton
JCGG-STR032526
Reactant Type
 Alcohol
Mol
 1 equiv.
MOLECULE ID
 JCGG-COM0000032
Reactant Type
 activator
Mol
 1 equiv.
PRODUCT
MOLECULE ID
 JCGG-COM0000381 (Reaction Tree)
Product Type
 alpha
Yield
 80%
REACTION DETAIL
Reaction Time
 overnight
Reaction Temp
 room temp
Solvent
 PhH
Catalyst
 activator
Comment
 MS 4A was included in the solvent.
The reaction was sheltered from the light.
COMMENT
The PMID could not be found.
Only alpha was detected in the product.
The alpha/beta ratio was determined by 13C NMR spectroscopy.
REFERENCE
Reference Id
 REF-0000-000014
Source
 Bulletin of the Chemical Society of Japan, Vol. 67 (1994), No. 5 pp.1359-1366
Doi
 10.1246/bcsj.67.1359
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)