|
Glycan Syntheses |
JCGG ID |
JCGG-RAC0000306 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-000306
|
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Regist Date |
2012/06/21 15:22:34 | |||||||
| REACTANT | ||||||||
|
|
|
|||||||
Reactant Type |
1-C-methyl-D-glucopyranosyl dimetylphosphinothioate | |||||||
Mol |
1 equiv. | |||||||
|
|
|
|||||||
Reactant Type |
Trityl salt | |||||||
Mol |
0.10 equiv. | |||||||
|
|
|
|
||||||
Reactant Type |
Alcohol | |||||||
Mol |
1 equiv. | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
|
|
||||||
Product Type |
alpha | |||||||
Yield |
82%(alpha/beta=70/30) | |||||||
MOLECULE ID |
|
|
||||||
Product Type |
beta | |||||||
Yield |
82%(alpha/beta=70/30) | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
1 hour | |||||||
Reaction Temp |
room temp | |||||||
Solvent |
PhH | |||||||
Catalyst |
Trityl salt | |||||||
| COMMENT | ||||||||
| The PMID could not be found. | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000009 | |||||||
Source |
HETEROCYCLES, Vol. 79, 2009, pp. 163 - 194 | |||||||
Doi |
10.3987/REV-08-SR(D)4 | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
|
