|
Glycan Syntheses |
JCGG ID |
JCGG-RAC0000293 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-000293
|
|||||||
Regist Date |
2012/06/21 15:17:25 | |||||||
| REACTANT | ||||||||
|
|
|
|
||||||
Reactant Type |
Glycosyl donor | |||||||
Mol |
1 equiv. | |||||||
|
|
|
|||||||
Reactant Type |
Substrate | |||||||
Mol |
1 equiv. | |||||||
|
|
|
|||||||
Reactant Type |
Activator | |||||||
Mol |
1 equiv. | |||||||
|
|
|
|||||||
Reactant Type |
Activator | |||||||
Mol |
0.1 equiv. | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
|
|
|
|||||
Product Type |
beta | |||||||
Yield |
63%(alpha/beta=0/100) | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
16 hours | |||||||
Reaction Temp |
room temp | |||||||
Solvent |
PhH | |||||||
Catalyst |
Activator | |||||||
Comment |
MS 4A was included in the solvent. | |||||||
| COMMENT | ||||||||
| The PMID could not be found. | ||||||||
| Only beta was obtained. | ||||||||
| The alpha/beta ratio was determined by 13C NMR. | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000005 | |||||||
Source |
Chemistry Letters, Vol. 18 (1989), No. 1 p.69 | |||||||
Doi |
10.1246/cl.1989.69 | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
|
