JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000288
Submitter
The Noguchi Institute
Reaction ID
R-0000-000288
Regist Date
2012/06/21 15:17:10
REACTANT
MOLECULE ID
JCGG-COM0000054 (Reaction Tree)
Reactant Type
1-Hydroxy sugar
Mol
1
MOLECULE ID
JCGG-COM0000231
Reactant Type
Activator
Mol
0.50
PRODUCT
MOLECULE ID
JCGG-COM0000309 (Reaction Tree)
Yield
23%
REACTION DETAIL
Reaction Time
1 day
Reaction Temp
room temp
Solvent
CH2Cl2
Catalyst
Activator
Comment
anhydrous CaSO4 was included in the solvent.
Scheme 2
COMMENT
The PMID could not be found.
The alpha/beta ratio was determined by NMR.
REFERENCE
Reference Id
REF-0000-000012
Source
HETEROCYCLES, Vol. 77, No. 1, 2009, pp. 445 - 460
Doi
10.3987/COM-08-S(F)41

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)