JCGG ID |
JCGG-RAC0000207 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000207 | ||||
Regist Date |
2012/06/21 14:52:45 | ||||
REACTANT | |||||
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|
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Reactant Type |
Donor[1,3,4,6-tetra-O-benzyl-D-frucofuranosyl acetate (alpha/beta=1/2)] | ||||
Mol |
1 | ||||
|
|
||||
Reactant Type |
Activator | ||||
Mol |
0.05 | ||||
|
|
||||
Reactant Type |
Acceptor | ||||
Mol |
1 | ||||
PRODUCT | |||||
MOLECULE ID |
|
|
|||
Product Type |
alpha | ||||
Yield |
92%(alpha/beta=65/35) | ||||
MOLECULE ID |
|
|
|||
Product Type |
beta | ||||
Yield |
92%(alpha/beta=65/35) | ||||
REACTION DETAIL | |||||
Reaction Time |
0.5 hour to overnight | ||||
Reaction Temp |
0 degree C | ||||
Solvent |
PhCH3 | ||||
Catalyst |
Activator | ||||
Comment |
Anhydrous CaSO4 was included in the solvent. | ||||
COMMENT | |||||
The PMID could not be found. | |||||
REFERENCE | |||||
Reference Id |
REF-0000-000011 | ||||
Source |
Tetrahedron Letters 48 (2007) 6458‐6462 | ||||
Doi |
10.1016/j.tetlet.2007.07.092 |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |