JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000201
Submitter
The Noguchi Institute
Reaction ID
R-0000-000201
Regist Date
2012/06/21 14:52:28
REACTANT
MOLECULE ID
JCGG-COM0000236 (Reaction Tree)
Reactant Type
1,3,4,6-tetra-O-benzoyl-D-fructofuranosyl acetate (alpha/beta=3/1)
Mol
1
MOLECULE ID
JCGG-COM0000006
Reactant Type
Lewis acid(activator)
Mol
0.05
MOLECULE ID
JCGG-COM0000096
Mol
1
PRODUCT
MOLECULE ID
JCGG-COM0000237 (Reaction Tree)
Product Type
alpha
Yield
trace
MOLECULE ID
JCGG-COM0000238 (Reaction Tree)
Product Type
beta
Yield
trace
REACTION DETAIL
Reaction Time
0.5 to 2 hours
Reaction Temp
0 degree C
Solvent
PhCH3
Catalyst
activator
Comment
Anhydrous CaSO4 was included in the solvent.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000011
Source
Tetrahedron Letters 48 (2007) 6458‐6462
Doi
10.1016/j.tetlet.2007.07.092

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)