JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000165
Submitter
The Noguchi Institute
Reaction ID
R-0000-000165
Regist Date
2012/06/21 14:37:37
REACTANT
MOLECULE ID
JCGG-COM0000115 (Reaction Tree)
Reactant Type
Ketose
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000186
Reactant Type
Nucleophile
Mol
3 equiv.
MOLECULE ID
JCGG-COM0000097
Reactant Type
activator
Mol
0.2 equiv.
PRODUCT
MOLECULE ID
JCGG-COM0000203 (Reaction Tree)
Yield
94% to 99%
REACTION DETAIL
Reaction Time
2 to 3 hours
Reaction Temp
-40 degree C
Solvent
MeCN
Catalyst
activator
Comment
CaSO4 was added to the solvent as a drying agent.
COMMENT
The PMID could not be found.
The alpha/beta ratio was NOT specified.
REFERENCE
Reference Id
REF-0000-000009
Source
HETEROCYCLES, Vol. 79, 2009, pp. 163 - 194
Doi
10.3987/REV-08-SR(D)4

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)