JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000136
Submitter
The Noguchi Institute
Reaction ID
R-0000-000136
Regist Date
2012/06/21 14:30:43
REACTANT
MOLECULE ID
JCGG-COM0000167 (Reaction Tree)
Reactant Type
Starting material
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000160
Mol
44 equiv.
MOLECULE ID
JCGG-COM0000161
Mol
15 equiv.
PRODUCT
MOLECULE ID
JCGG-COM0000168 (Reaction Tree)
Yield
78%
REACTION DETAIL
Reaction Time
overnight
Reaction Temp
room temp
Solvent
DMF
Comment
The reactants were mixed at 0 degree in Celsius before stirred at room temperature.
COMMENT
The alpha/beta ratio was NOT specified.
5 Hydrate was used.
REFERENCE
Reference Id
REF-0000-000007
Issn
Print
Doi
10.1016/j.carres.2008.03.024
PubMed ID
18423585
Journal Name
Carbohydrate research. (2008) 343 (8): 1366-72.
Article Title
Preparation of partially benzylated mono-, di-, and trisaccharides by selective cleavage of the beta-fructofuranosidic linkage in fully benzylated sucrose and sucrose-related oligosaccharides under acidic conditions.
Author
Takashi, Yamanoi; Noriko, Misawa; Sho, Matsuda; Mikio, Watanabe
Affiliation
The Noguchi Institute, Tokyo, Japan. tyama@noguchi.or.jp
Reference Id
REF-0000-000008
Source
Carbohydrate Research 343 (2008) 1366‐1372
Doi
10.1016/j.carres.2008.03.024

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)