JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000127
Submitter
The Noguchi Institute
Reaction ID
R-0000-000127
Regist Date
2012/06/21 14:30:15
REACTANT
MOLECULE ID
JCGG-COM0000136 (Reaction Tree)
Reactant Type
donor
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000043 (Reaction Tree)
Skeleton
JCGG-STR032526
Reactant Type
Acceptor
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000084
Reactant Type
Activator
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000035
Reactant Type
Activator
Mol
0.05 equiv.
PRODUCT
MOLECULE ID
JCGG-COM0000145 (Reaction Tree)
Skeleton
JCGG-STR005997
Product Type
alpha
Yield
69%(alpha/beta=50/50)
MOLECULE ID
JCGG-COM0000146 (Reaction Tree)
Product Type
beta
Yield
69%(alpha/beta=50/50)
REACTION DETAIL
Solvent
PhH
Catalyst
Activator
Comment
MS 4A was included in the solvent.
The reaction temperature could not be found.
The reaction time could not be found.
COMMENT
The PMID could not be found.
The alpha/beta ratio was determined by HPLC and 1H NMR.
REFERENCE
Reference Id
REF-0000-000006
Source
Chemistry Letters Vol. 22 (1993), No. 2 p.343
Doi
10.1246/cl.1993.343

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)