JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000050
Submitter
The Noguchi Institute
Reaction ID
R-0000-000050
Regist Date
2012/06/21 12:46:39
REACTANT
MOLECULE ID
JCGG-COM0000048 (Reaction Tree)
Skeleton
JCGG-STR032525
Reactant Type
Donor
Mol
0.2 mmol
MOLECULE ID
JCGG-COM0000031
Reactant Type
Acceptor
Mol
0.2 mmol
MOLECULE ID
JCGG-COM0000032
Mol
0.2 mmol
PRODUCT
MOLECULE ID
JCGG-COM0000063 (Reaction Tree)
Skeleton
JCGG-STR032525
Product Type
alpha
Yield
89%(alpha/beta=81/19)
MOLECULE ID
JCGG-COM0000064 (Reaction Tree)
Skeleton
JCGG-STR031569
Product Type
beta
Yield
89%(alpha/beta=81/19)
REACTION DETAIL
Reaction Time
overnight
Solvent
benzene
Catalyst
AgClO4
Comment
MS 4A was included in the solvent.
The reaction temperature could not be found. (considered to be room temp)
COMMENT
The PMID could not be found.
The alpha/beta ratio was determined by isolated yield.
REFERENCE
Reference Id
REF-0000-000003
Source
Bull. Chem. Soc. Jpn., 66, 2617-2622 (1993)
Doi
10.1246/bcsj.66.2617

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)