JCGG ID |
JCGG-RAC0000046 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-000046 | |||||||
Regist Date |
2012/06/21 12:46:27 | |||||||
REACTANT | ||||||||
|
|
|||||||
Reactant Type |
Compound | |||||||
Mol |
5.0 mmol | |||||||
|
|
|||||||
Reactant Type |
Base | |||||||
Mol |
5.5 mmol | |||||||
|
|
|||||||
Mol |
5.5 mmol | |||||||
PRODUCT | ||||||||
MOLECULE ID |
|
|
|
|||||
Product Type |
alpha | |||||||
Yield |
90%(alpha/beta=86/14) | |||||||
MOLECULE ID |
|
|
||||||
Product Type |
beta | |||||||
Yield |
90%(alpha/beta=86/14) | |||||||
REACTION DETAIL | ||||||||
Reaction Time |
1 hour | |||||||
Reaction Temp |
-30 degree C | |||||||
Solvent |
THF | |||||||
COMMENT | ||||||||
The PMID could not be found. | ||||||||
The alpha/beta ratio was determined by 1H NMR spectra. | ||||||||
REFERENCE | ||||||||
Reference Id |
REF-0000-000003 | |||||||
Source |
Bull. Chem. Soc. Jpn., 66, 2617-2622 (1993) | |||||||
Doi |
10.1246/bcsj.66.2617 |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |