JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000043
Submitter
The Noguchi Institute
Reaction ID
R-0000-000043
Regist Date
2012/06/21 12:46:18
REACTANT
MOLECULE ID
JCGG-COM0000046 (Reaction Tree)
Reactant Type
Compound
Mol
5.0 mmol
MOLECULE ID
JCGG-COM0000028
Reactant Type
Base
Mol
5.5 mmol
MOLECULE ID
JCGG-COM0000029
Mol
5.5 mmol
PRODUCT
MOLECULE ID
JCGG-COM0000048 (Reaction Tree)
Skeleton
JCGG-STR032525
Product Type
alpha
Yield
96%(alpha/beta=98/2)
MOLECULE ID
JCGG-COM0000049 (Reaction Tree)
Skeleton
JCGG-STR031569
Product Type
beta
Yield
96%(alpha/beta=98/2)
REACTION DETAIL
Reaction Time
1 hour
Reaction Temp
-30 degree C
Solvent
THF
COMMENT
The PMID could not be found.
The alpha/beta ratio was determined by 1H NMR spectra.
REFERENCE
Reference Id
REF-0000-000003
Source
Bull. Chem. Soc. Jpn., 66, 2617-2622 (1993)
Doi
10.1246/bcsj.66.2617

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)