JCGG ID |
JCGG-RAC0000040 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-000040 | |||||||
Regist Date |
2012/06/21 12:26:43 | |||||||
REACTANT | ||||||||
|
|
|||||||
Mol |
1 equiv. | |||||||
|
|
|
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Reactant Type |
Alcohol | |||||||
Mol |
1 equiv. | |||||||
|
|
|||||||
Reactant Type |
Activator | |||||||
Mol |
0.3 equiv. | |||||||
PRODUCT | ||||||||
MOLECULE ID |
|
|
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Product Type |
alpha | |||||||
Yield |
62%(alpha/beta=8/1) | |||||||
MOLECULE ID |
|
|
||||||
Product Type |
beta | |||||||
Yield |
62%(alpha/beta=8/1) | |||||||
REACTION DETAIL | ||||||||
Reaction Time |
2 hours | |||||||
Reaction Temp |
room temp | |||||||
Solvent |
PhH | |||||||
Catalyst |
Activator | |||||||
Comment |
MS 4A was included in the solvent. | |||||||
COMMENT | ||||||||
The PMID could not be found. | ||||||||
The alpha/beta ratio was determined by 13C NMR spectroscopy. | ||||||||
REFERENCE | ||||||||
Reference Id |
REF-0000-000002 | |||||||
Source |
CHEMISTRY LETTERS, pp. 849-852, 1990 | |||||||
Doi |
10.1246/cl.1990.849 |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |