Reaction:JCGG-RAC0000038

JCGG ID		JCGG-RAC0000038
Submitter		The Noguchi Institute
Reaction ID		R-0000-000038
Regist Date		2012/06/21 12:26:36
REACTANT
MOLECULE ID		JCGG-COM0000030 (Reaction Tree)
	Mol	1 equiv.
MOLECULE ID		JCGG-COM0000037
	Reactant Type	Alcohol
	Mol	1 equiv.
MOLECULE ID		JCGG-COM0000035
	Reactant Type	Activator
	Mol	0.3 equiv.
PRODUCT
MOLECULE ID		JCGG-COM0000038 (Reaction Tree)
	Product Type	alpha
	Yield	64%(alpha/beta=12/1)
MOLECULE ID		JCGG-COM0000039 (Reaction Tree)
	Product Type	beta
	Yield	64%(alpha/beta=12/1)
REACTION DETAIL
Reaction Time		2 hours
Reaction Temp		room temp
Solvent		PhH
Catalyst		Activator
Comment		MS 4A was included in the solvent.
COMMENT
The PMID could not be found.
The alpha/beta ratio was determined by 13C NMR spectroscopy.
REFERENCE
Reference Id		REF-0000-000002
	Source	CHEMISTRY LETTERS, pp. 849-852, 1990
	Doi	10.1246/cl.1990.849