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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000035 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000035
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Regist Date |
2012/06/21 12:26:27 | ||||
| REACTANT | |||||
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Mol |
1 equiv. | ||||
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Reactant Type |
ROH | ||||
Mol |
1 equiv. | ||||
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Reactant Type |
Activator | ||||
Mol |
0.3 equiv. | ||||
| PRODUCT | |||||
MOLECULE ID |
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Product Type |
alpha | ||||
Yield |
62%(alpha/beta=5/1) | ||||
MOLECULE ID |
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Product Type |
beta | ||||
Yield |
62%(alpha/beta=5/1) | ||||
| REACTION DETAIL | |||||
Reaction Time |
2 hours | ||||
Reaction Temp |
room temp | ||||
Solvent |
CH2Cl2 | ||||
Catalyst |
Activator | ||||
Comment |
MS 4A was included in the solvent. | ||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| The alpha/beta ratio was determined by 13C NMR spectroscopy. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000002 | ||||
Source |
CHEMISTRY LETTERS, pp. 849-852, 1990 | ||||
Doi |
10.1246/cl.1990.849 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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