JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000017
Submitter
The Noguchi Institute
Reaction ID
R-0000-000017
Regist Date
2012/06/21 11:56:49
REACTANT
MOLECULE ID
JCGG-COM0000001 (Reaction Tree)
Skeleton
JCGG-STR032527
Mol
1
MOLECULE ID
JCGG-COM0000002
Reactant Type
activator
Mol
0.02
MOLECULE ID
JCGG-COM0000003
Mol
0.50
PRODUCT
MOLECULE ID
JCGG-COM0000004 (Reaction Tree)
Skeleton
JCGG-STR032527
Yield
86%(alpha/beta=100/0)
REACTION DETAIL
Reaction Time
1.5 hours
Reaction Temp
0 degree C
Solvent
CH2Cl2
Catalyst
activator
Comment
CaSO4 was added to the solvent as a drying agent.
COMMENT
The PMID could not be found.
Only alpha was detected in the product.
REFERENCE
Reference Id
REF-0000-000001
Source
Tetrahedron Letters 42 (2001) 4009‐4011
Doi
10.1016/S0040-4039(01)00644-X

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