JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000016
Submitter
The Noguchi Institute
Reaction ID
R-0000-000016
Regist Date
2012/06/21 11:56:46
REACTANT
MOLECULE ID
JCGG-COM0000001 (Reaction Tree)
Skeleton
JCGG-STR032527
Mol
1
MOLECULE ID
JCGG-COM0000002
Reactant Type
activator
Mol
0.04
MOLECULE ID
JCGG-COM0000010
Mol
0.50
PRODUCT
MOLECULE ID
JCGG-COM0000011 (Reaction Tree)
Skeleton
JCGG-STR032527
Yield
61%(alpha/beta=100/0)
REACTION DETAIL
Reaction Time
5 hours
Reaction Temp
0 degree C
Solvent
CH2Cl2
Catalyst
activator
Comment
CaSO4 was added to the solvent as a drying agent.
COMMENT
The PMID could not be found.
Only alpha was detected in the product.
REFERENCE
Reference Id
REF-0000-000001
Source
Tetrahedron Letters 42 (2001) 4009‐4011
Doi
10.1016/S0040-4039(01)00644-X

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